#FILE: x #FORMAT: x #IDENTITY: x #DECIMAL: x #SEPARATOR: x #MTYPE: DSC #MSUBTYPE: #INSTRUMENT: x #PROJECT: x #DATE/TIME: x #CORR. FILE: #LABORATORY: HS Merseburg #OPERATOR: x #REMARK: #SAMPLE: x #SAMPLE MASS /mg: 20,000 #MATERIAL: x #REFERENCE: x #REFERENCE MASS /mg: x #TYPE OF CRUCIBLE: x #SAMPLE CRUCIBLE MASS /mg: x #REFERENCE CRUCIBLE MASS /mg: x #PROTECTIVE GAS: x #FLOW RATE: #PURGE GAS 1: x #FLOW RATE 1 /(ml/min): x #PURGE GAS 2: x #FLOW RATE 2 /(ml/min): x #CORR. CODE: x #EXO: x #RANGE: x #SEGMENT: x ##Temp./ C Time/min DSC/(mW/mg) Sensit./( V/mW) 30,55700 0,0000e+000 -8,2124e-002 3,46084 30,53619 2,5042e-002 -7,2764e-002 3,46071 30,51145 5,0083e-002 -6,5679e-002 3,46055 30,48474 7,5125e-002 -5,9111e-002 3,46038 30,46443 0,10017 -5,2475e-002 3,46025 30,45107 0,12521 -4,6607e-002 3,46017 30,43668 0,15025 -4,1277e-002 3,46008 30,42276 0,17529 -3,6326e-002 3,45999 30,40693 0,20033 -3,1709e-002 3,45984 30,38973 0,22538 -2,7627e-002 3,45978 30,37256 0,25042 -2,3998e-002 3,45967 30,35522 0,27546 -2,0641e-002 3,45956 30,33780 0,30050 -1,7591e-002 3,45945 30,32249 0,32554 -1,4852e-002 3,45935 30,30926 0,35058 -1,2343e-002 3,45921 30,29756 0,37563 -1,0159e-002 3,45919 30,28520 0,40067 -8,2846e-003 3,45911 30,27146 0,42571 -6,5246e-003 3,45902 30,25750 0,45075 -4,8029e-003 3,45893 30,24228 0,47579 -3,2997e-003 3,45884 30,22601 0,50083 -1,9625e-003 3,45873 30,21000 0,52588 -8,4885e-004 3,45863 30,19362 0,55092 1,3301e-004 3,45853 30,17613 0,57596 1,0386e-003 3,45841 30,15924 0,60100 1,8384e-003 3,45831 30,14474 0,62604 2,6555e-003 3,45821 30,13063 0,65108 3,2432e-003 3,45812 30,11700 0,67613 3,7855e-003 3,45804 30,10431 0,70117 4,2639e-003 3,45793 30,09162 0,72621 4,5877e-003 3,45787 30,07760 0,75125 4,9359e-003 3,45778 30,06197 0,77629 5,3749e-003 3,45769 30,04505 0,80133 5,5667e-003 3,45758 30,02789 0,82638 5,7500e-003 3,45747 30,01221 0,85142 6,0390e-003 3,45737 29,99793 0,87646 6,2577e-003 3,45728 29,98392 0,90150 6,3452e-003 3,45719 29,97118 0,92654 6,4455e-003 3,45710 29,95985 0,95158 6,5073e-003 3,45703 29,95016 0,97663 6,5225e-003 3,45697 29,94163 1,00167 6,5510e-003 3,45692 29,93262 1,02671 6,5647e-003 3,45686 29,92226 1,05175 6,5128e-003 3,45679 29,91175 1,07679 6,4638e-003 3,45672 29,90118 1,10183 6,3623e-003 3,45665 29,89069 1,12688 6,3731e-003 3,45659 29,88104 1,15192 6,2387e-003 3,45653 29,87265 1,17696 6,0337e-003 3,45647 29,86564 1,20200 6,0882e-003 3,45643 29,86031 1,22704 6,0355e-003 3,45640 29,85528 1,25208 5,8507e-003 3,45636 29,84898 1,27713 5,7547e-003 3,45632 29,84205 1,30217 5,6579e-003 3,45628 29,83415 1,32721 5,5546e-003 3,45623 29,82428 1,35225 5,5190e-003 3,45616 29,81393 1,37729 5,3202e-003 3,45610 29,80345 1,40233 5,0953e-003 3,45601 29,79282 1,42738 5,0341e-003 3,45596 29,78275 1,45242 4,9248e-003 3,45590 29,77417 1,47746 4,7717e-003 3,45584 29,76696 1,50250 4,7732e-003 3,45580 29,75995 1,52754 4,7199e-003 3,45575 29,75280 1,55258 4,5621e-003 3,45571 29,74383 1,57763 4,4825e-003 3,45565 29,73358 1,60267 4,4217e-003 3,45558 29,72320 1,62771 4,2620e-003 3,45552 29,71270 1,65275 4,0676e-003 3,45545 29,70223 1,67779 3,9415e-003 3,45537 29,69274 1,70283 3,8424e-003 3,45532 29,68496 1,72788 3,7615e-003 3,45527 29,67787 1,75292 3,6110e-003 3,45523 29,67179 1,77796 3,5251e-003 3,45519 29,66770 1,80300 3,5239e-003 3,45516 29,66405 1,82804 3,2969e-003 3,45514 29,65923 1,85308 3,2025e-003 3,45511 29,65282 1,87813 3,2024e-003 3,45507 29,64595 1,90317 3,1135e-003 3,45502 29,63869 1,92821 3,0171e-003 3,45498 29,63015 1,95325 3,0147e-003 3,45492 29,62043 1,97829 2,9328e-003 3,45486 29,61033 2,00333 2,7772e-003 3,45479 29,60192 2,02838 2,7020e-003 3,45473 29,59470 2,05342 2,6743e-003 3,45469 29,58762 2,07846 2,5916e-003 3,45465 29,58062 2,10350 2,4536e-003 3,45460 29,57361 2,12854 2,3524e-003 3,45456 29,56661 2,15358 2,3425e-003 3,45451 29,55948 2,17863 2,2184e-003 3,45447 29,55201 2,20367 2,0390e-003 3,45442 29,54448 2,22871 2,0172e-003 3,45437 29,53650 2,25375 2,0645e-003 3,45432 29,52736 2,27879 1,9242e-003 3,45426 29,51923 2,30383 1,8628e-003 3,45421 29,51247 2,32888 1,8603e-003 3,45417 29,50565 2,35392 1,7887e-003 3,45409 29,49892 2,37896 1,7103e-003 3,45408 29,49349 2,40400 1,6948e-003 3,45405 29,48922 2,42904 1,6451e-003 3,45402 29,48551 2,45408 1,5875e-003 3,45399 29,48198 2,47913 1,4878e-003 3,45397 29,47848 2,50417 1,3830e-003 3,45395 29,47498 2,52921 1,4349e-003 3,45393 29,47146 2,55425 1,5455e-003 3,45390 29,46777 2,57929 1,4210e-003 3,45388 29,46380 2,60433 1,3123e-003 3,45386 29,45896 2,62938 1,2249e-003 3,45382 29,45314 2,65442 1,2122e-003 3,45379 29,44677 2,67946 1,2480e-003 3,45375 29,44082 2,70450 1,2369e-003 3,45371 29,43601 2,72954 1,1758e-003 3,45368 29,43197 2,75458 1,1076e-003 3,45365 29,42948 2,77963 1,0952e-003 3,45363 29,42876 2,80467 1,1424e-003 3,45363 29,42851 2,82971 1,0773e-003 3,45363 29,42895 2,85475 9,5346e-004 3,45363 29,43184 2,87979 9,5283e-004 3,45365 29,43627 2,90483 6,8573e-004 3,45368 29,44453 2,92988 3,2370e-004 3,45373 29,45628 2,95492 -3,0594e-004 3,45381 29,47201 2,97996 -1,4975e-003 3,45391 29,49312 3,00500 -3,5313e-003 3,45404 29,52012 3,03004 -6,6501e-003 3,45422 29,55394 3,05508 -1,0887e-002 3,45443 29,59485 3,08013 -1,6578e-002 3,45470 29,64381 3,10517 -2,3564e-002 3,45501 29,70100 3,13021 -3,1812e-002 3,45537 29,76612 3,15525 -4,1349e-002 3,45579 29,83944 3,18029 -5,1916e-002 3,45626 29,92088 3,20533 -6,3325e-002 3,45678 30,00947 3,23038 -7,5563e-002 3,45729 30,10533 3,25542 -8,8240e-002 3,45793 30,21027 3,28046 -0,10098 3,45863 30,32413 3,30550 -0,11378 3,45936 30,44503 3,33054 -0,12658 3,46013 30,57376 3,35558 -0,13897 3,46095 30,70858 3,38063 -0,15110 3,46175 30,84987 3,40567 -0,16279 3,46271 30,99668 3,43071 -0,17393 3,46364 31,14731 3,45575 -0,18455 3,46460 31,30168 3,48079 -0,19432 3,46557 31,46015 3,50583 -0,20299 3,46658 31,62284 3,53088 -0,21157 3,46761 31,78910 3,55592 -0,21966 3,46866 31,95717 3,58096 -0,22704 3,46972 32,12663 3,60600 -0,23391 3,47079 32,29845 3,63104 -0,24020 3,47188 32,47196 3,65608 -0,24589 3,47297 32,64745 3,68113 -0,25109 3,47407 32,82452 3,70617 -0,25581 3,47519 33,00222 3,73121 -0,26014 3,47629 33,18009 3,75625 -0,26406 3,47742 33,35842 3,78129 -0,26751 3,47853 33,53723 3,80633 -0,27074 3,47965 33,71583 3,83138 -0,27361 3,48077 33,89450 3,85642 -0,27614 3,48188 34,07324 3,88146 -0,27834 3,48299 34,25279 3,90650 -0,28019 3,48411 34,43374 3,93154 -0,28179 3,48524 34,61423 3,95658 -0,28327 3,48636 34,79408 3,98163 -0,28455 3,48747 34,97397 4,00667 -0,28560 3,48859 35,15450 4,03171 -0,28651 3,48970 35,33515 4,05675 -0,28731 3,49082 35,51481 4,08179 -0,28800 3,49193 35,69344 4,10683 -0,28862 3,49303 35,87173 4,13188 -0,28897 3,49413 36,04944 4,15692 -0,28920 3,49522 36,22687 4,18196 -0,28947 3,49631 36,40420 4,20700 -0,28974 3,49737 36,58123 4,23204 -0,28988 3,49848 36,75815 4,25708 -0,28994 3,49957 36,93460 4,28213 -0,28995 3,50065 37,11035 4,30717 -0,28988 3,50172 37,28645 4,33221 -0,28975 3,50279 37,46233 4,35725 -0,28967 3,50386 37,63641 4,38229 -0,28964 3,50492 37,80978 4,40733 -0,28944 3,50592 37,98349 4,43238 -0,28917 3,50703 38,15588 4,45742 -0,28897 3,50808 38,32721 4,48246 -0,28868 3,50911 38,49769 4,50750 -0,28832 3,51015 38,66740 4,53254 -0,28805 3,51117 38,83786 4,55758 -0,28778 3,51220 39,00713 4,58263 -0,28741 3,51318 39,17574 4,60767 -0,28703 3,51423 39,34420 4,63271 -0,28667 3,51525 39,51216 4,65775 -0,28637 3,51626 39,67934 4,68279 -0,28610 3,51726 39,84583 4,70783 -0,28576 3,51826 40,01171 4,73288 -0,28542 3,51925 40,17743 4,75792 -0,28507 3,52024 40,34221 4,78296 -0,28483 3,52123 40,50606 4,80800 -0,28461 3,52217 40,66963 4,83304 -0,28427 3,52318 40,83211 4,85808 -0,28403 3,52414 40,99276 4,88313 -0,28373 3,52510 41,15310 4,90817 -0,28345 3,52605 41,31375 4,93321 -0,28319 3,52700 41,47421 4,95825 -0,28288 3,52796 41,63404 4,98329 -0,28257 3,52890 41,79317 5,00833 -0,28233 3,52984 41,95174 5,03338 -0,28205 3,53078 42,11066 5,05842 -0,28171 3,53172 42,26895 5,08346 -0,28146 3,53265 42,42620 5,10850 -0,28120 3,53357 42,58301 5,13354 -0,28081 3,53450 42,73918 5,15858 -0,28055 3,53541 42,89487 5,18363 -0,28030 3,53633 43,04989 5,20867 -0,28010 3,53723 43,20467 5,23371 -0,27984 3,53811 43,35903 5,25875 -0,27954 3,53904 43,51273 5,28379 -0,27934 3,53994 43,66656 5,30883 -0,27919 3,54084 43,82087 5,33388 -0,27889 3,54174 43,97533 5,35892 -0,27856 3,54264 44,12894 5,38396 -0,27839 3,54353 44,28209 5,40900 -0,27824 3,54442 44,43508 5,43404 -0,27795 3,54531 44,58704 5,45908 -0,27764 3,54619 44,73911 5,48413 -0,27748 3,54707 44,89068 5,50917 -0,27734 3,54794 45,04203 5,53421 -0,27707 3,54882 45,19346 5,55925 -0,27686 3,54969 45,34470 5,58429 -0,27681 3,55056 45,49547 5,60933 -0,27669 3,55143 45,64529 5,63438 -0,27651 3,55229 45,79405 5,65942 -0,27626 3,55315 45,94130 5,68446 -0,27604 3,55399 46,08897 5,70950 -0,27595 3,55484 46,23777 5,73454 -0,27583 3,55569 46,38541 5,75958 -0,27560 3,55653 46,53265 5,78463 -0,27559 3,55737 46,67836 5,80967 -0,27551 3,55821 46,82433 5,83471 -0,27531 3,55904 46,97119 5,85975 -0,27517 3,55987 47,11792 5,88479 -0,27507 3,56071 47,26417 5,90983 -0,27491 3,56154 47,40956 5,93488 -0,27476 3,56231 47,55472 5,95992 -0,27466 3,56319 47,69968 5,98496 -0,27451 3,56401 47,84432 6,01000 -0,27431 3,56483 47,98829 6,03504 -0,27426 3,56564 48,13168 6,06008 -0,27440 3,56645 48,27604 6,08513 -0,27431 3,56726 48,42081 6,11017 -0,27417 3,56808 48,56672 6,13521 -0,27421 3,56890 48,71188 6,16025 -0,27424 3,56972 48,85534 6,18529 -0,27417 3,57052 48,99918 6,21033 -0,27420 3,57133 49,14296 6,23538 -0,27426 3,57213 49,28757 6,26042 -0,27433 3,57294 49,43127 6,28546 -0,27427 3,57375 49,57380 6,31050 -0,27422 3,57454 49,71626 6,33554 -0,27428 3,57534 49,85886 6,36058 -0,27426 3,57613 50,00168 6,38563 -0,27418 3,57692 50,14401 6,41067 -0,27410 3,57772 50,28534 6,43571 -0,27405 3,57850 50,42662 6,46075 -0,27397 3,57929 50,56860 6,48579 -0,27390 3,58007 50,71029 6,51083 -0,27391 3,58086 50,85101 6,53588 -0,27389 3,58163 50,99284 6,56092 -0,27379 3,58242 51,13402 6,58596 -0,27371 3,58320 51,27452 6,61100 -0,27362 3,58397 51,41561 6,63604 -0,27357 3,58475 51,55632 6,66108 -0,27363 3,58552 51,69516 6,68613 -0,27364 3,58628 51,83318 6,71117 -0,27358 3,58704 51,97166 6,73621 -0,27349 3,58780 52,11030 6,76125 -0,27344 3,58856 52,24836 6,78629 -0,27343 3,58932 52,38584 6,81133 -0,27338 3,59007 52,52305 6,83638 -0,27340 3,59082 52,66069 6,86142 -0,27335 3,59157 52,79878 6,88646 -0,27339 3,59232 52,93599 6,91150 -0,27344 3,59306 53,07194 6,93654 -0,27347 3,59380 53,20835 6,96158 -0,27356 3,59450 53,34605 6,98663 -0,27361 3,59529 53,48239 7,01167 -0,27370 3,59603 53,61849 7,03671 -0,27375 3,59677 53,75453 7,06175 -0,27378 3,59750 53,88998 7,08679 -0,27391 3,59823 54,02587 7,11183 -0,27410 3,59897 54,16306 7,13688 -0,27418 3,59970 54,30012 7,16192 -0,27416 3,60044 54,43643 7,18696 -0,27415 3,60118 54,57268 7,21200 -0,27425 3,60191 54,70879 7,23704 -0,27440 3,60259 54,84460 7,26208 -0,27445 3,60337 54,98070 7,28713 -0,27450 3,60409 55,11452 7,31217 -0,27467 3,60481 55,24815 7,33721 -0,27475 3,60552 55,38225 7,36225 -0,27485 3,60624 55,51621 7,38729 -0,27503 3,60695 55,65006 7,41233 -0,27522 3,60767 55,78372 7,43738 -0,27544 3,60838 55,91744 7,46242 -0,27565 3,60909 56,05037 7,48746 -0,27586 3,60979 56,18341 7,51250 -0,27608 3,61050 56,31703 7,53754 -0,27639 3,61121 56,44999 7,56258 -0,27675 3,61191 56,58184 7,58763 -0,27700 3,61261 56,71372 7,61267 -0,27750 3,61330 56,84550 7,63771 -0,27788 3,61400 56,97764 7,66275 -0,27813 3,61469 57,10999 7,68779 -0,27842 3,61534 57,24158 7,71283 -0,27876 3,61608 57,37281 7,73788 -0,27913 3,61677 57,50529 7,76292 -0,27948 3,61744 57,63715 7,78796 -0,27974 3,61815 57,76894 7,81300 -0,28004 3,61884 57,90101 7,83804 -0,28052 3,61953 58,03243 7,86308 -0,28100 3,62022 58,16347 7,88813 -0,28128 3,62090 58,29441 7,91317 -0,28174 3,62159 58,42666 7,93821 -0,28221 3,62228 58,55881 7,96325 -0,28274 3,62296 58,69003 7,98829 -0,28334 3,62364 58,82165 8,01333 -0,28387 3,62433 58,95403 8,03838 -0,28447 3,62501 59,08589 8,06342 -0,28518 3,62570 59,21817 8,08846 -0,28581 3,62638 59,34940 8,11350 -0,28647 3,62706 59,47990 8,13854 -0,28719 3,62773 59,61118 8,16358 -0,28786 3,62841 59,74222 8,18863 -0,28855 3,62908 59,87317 8,21367 -0,28945 3,62976 60,00444 8,23871 -0,29031 3,63041 60,13547 8,26375 -0,29130 3,63110 60,26631 8,28879 -0,29234 3,63177 60,39749 8,31383 -0,29327 3,63244 60,52889 8,33888 -0,29432 3,63312 60,66037 8,36392 -0,29537 3,63379 60,79097 8,38896 -0,29646 3,63445 60,92136 8,41400 -0,29756 3,63512 61,05191 8,43904 -0,29874 3,63578 61,18264 8,46408 -0,30004 3,63645 61,31401 8,48913 -0,30135 3,63712 61,44500 8,51417 -0,30281 3,63778 61,57530 8,53921 -0,30418 3,63844 61,70613 8,56425 -0,30563 3,63907 61,83771 8,58929 -0,30721 3,63977 61,96960 8,61433 -0,30877 3,64044 62,10177 8,63938 -0,31033 3,64109 62,23318 8,66442 -0,31194 3,64177 62,36361 8,68946 -0,31381 3,64242 62,49383 8,71450 -0,31574 3,64308 62,62374 8,73954 -0,31768 3,64373 62,75337 8,76458 -0,31977 3,64438 62,88346 8,78963 -0,32192 3,64503 63,01327 8,81467 -0,32427 3,64568 63,14330 8,83971 -0,32666 3,64633 63,27291 8,86475 -0,32923 3,64698 63,40267 8,88979 -0,33197 3,64761 63,53245 8,91483 -0,33477 3,64828 63,66103 8,93988 -0,33768 3,64892 63,79037 8,96492 -0,34076 3,64956 63,91919 8,98996 -0,34409 3,65020 64,04785 9,01500 -0,34786 3,65084 64,17624 9,04004 -0,35192 3,65147 64,30377 9,06508 -0,35606 3,65209 64,43083 9,09013 -0,36027 3,65273 64,55794 9,11517 -0,36452 3,65336 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